Recent advancements in micro/nanofabrication have introduced new techniques for creating and characterizing materials, enabling the study of transport phenomena across various engineering disciplines. Nanotechnology has shown significant potential, particularly in the development of micro/nanostructured surfaces for phase change heat transfer applications, such as boiling, evaporation, condensation, and freezing. These innovations are critical for high-heat-flux electronics cooling, desalination, and industrial power generation. Researchers have successfully controlled droplet nucleation on hybrid or biphilic surfaces, which combine hydrophobic and hydrophilic properties, enhancing fog harvesting, heat transfer, and icing prevention. However, current fabrication techniques face challenges, including scalability, high costs, and a lack of optimized design guidelines. My work focuses on developing scalable, efficient fabrication methods and improving numerical models to better predict the performance of these surfaces in phase change applications, ultimately contributing to improved energy efficiency in thermal systems.